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Blood 136 (4), 489500

1 H NMR (400 MHz, DMSO- d 6 ) 12.29 (s, 1H), 11.12 (s, 1H), 7.857.68 (m, 2H), 7.687.54 (m, 1H), 7.40 (d, J = 11.1 Hz, 1H), 6.72 (d, J = 5.0 Hz, 1H), 5.12 (dd, J = 12.7, 5.3 Hz, 1H), 4.33 (d, J = 11.9 Hz, 1H), 4.234.09 (m, 2H), 4.04 (d, J = 11.0 Hz, 2H), 3.84 (d, J = 13.3 Hz, 1H), 3.73 (t, J = 6.2 Hz, 2H), 3.643.45 (m, 6H), 2.99 (d, J = 12.8 Hz, 1H), 2.87 (d, J = 13.9 Hz, 1H), 2.73 (s, 1H), 2.60 (dd, J = 35.6, 16.8 Hz, 3H), 2.05 (d, J = 12.5 Hz, 1H), 1.81 (d, J = 12.0 Hz, 2H), 1.60 (d, J = 12.3 Hz, 1H), 1.43 (d, J = 9.8 Hz, 1H), 1.18 (d, J = 6.0 Hz, 9H)

However, provided variations in the water content within the sample are much smaller than the variations in the metabolite levels, variance shared between normalized metabolite signals can be assumed to arise largely from shared variance in metabolite concentrations [52]

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doi: 10.1080/07315724.2015.1031355

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